超清版 GB/T 44364-2024 牙膏中丙烯酰胺的测定 高效液相色谱串联质谱法
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资料介绍
ICS 71.100.40
CCS Y 43
中华人民共和国国家标准
GB/T 44364—2024
牙膏中丙烯酰胺的测定 高效液相色谱串联质谱法
Determination of acrylamide in toothpaste—
High performance liquid chromatography tandem mass spectrometry
2024-08-23 发布2025-03-01 实施
国家市场监督管理总局
国家标准化管理委员会发 布
目 次
前言 ····································································································· Ⅲ
1 范围 ·································································································· 1
2 规范性引用文件 ······················································································ 1
3 术语和定义 ··························································································· 1
4 原理 ·································································································· 1
5 试剂和材料 ··························································································· 1
6 仪器设备 ······························································································ 2
7 试验步骤 ······························································································ 2
7.1 试样溶液的制备 ················································································· 2
7.2 测定 ······························································································ 2
7.3 标准工作曲线绘制 ··············································································· 3
7.4 试样测定 ························································································· 3
7.5 空白试验 ························································································· 4
8 结果计算 ······························································································ 4
9 回收率 ································································································ 4
10 精密度 ······························································································· 4
11 检测限和定量限 ····················································································· 4
附录A （资料性） 丙烯酰胺标准物质/标准样品及内标信息 ·········································· 5
附录B （资料性） 丙烯酰胺及其内标标准溶液的多反应监测色谱图 ································· 6
前 言
本文件按照GB/T 1.1—2020《标准化工作导则 第1 部分：标准化文件的结构和起草规则》的规
定起草。
请注意本文件的某些内容可能涉及专利。本文件的发布机构不承担识别专利的责任。
本文件由中国轻工业联合会提出。
本文件由全国口腔护理用品标准化技术委员会（SAC/TC 492）归口。
本文件起草单位：苏州世谱检测技术有限公司、苏科世谱生物技术（苏州）有限公司、苏州质量检
测科学研究院、苏州市科耐瑞检测技术有限公司、广州舒客实业有限公司、广州质量监督检测研究院、
黑龙江省轻工科学研究院、无限极（中国）有限公司、福建爱洁丽日化有限公司、柳州两面针股份有限
公司、重庆登康口腔护理用品股份有限公司、浙江方圆检测集团股份有限公司、河北省食品检验研究
院、江苏省产品质量监督检验研究院、江苏省食品药品监督检验研究院、完美（广东）日用品有限公
司、清华大学、深圳大学、海南大学、苏州大学、常州大学、常州市食品药品纤维质量监督检验中心、
苏州市药品检验检测研究中心、山东华素健康护理品有限公司。
本文件主要起草人：张岩、卢剑、方方、何霜、朱丹丹、郑卫、结莉、李建祥、刘斌、秦天依、
叶竹洪、刘文玉、陈敏珊、高艳、蔡丽萍、胡永志、张环、杨铭、肖俊芳、代丹、陈晓珍、郭新东、
王怡、黄金凤、张迎阳、黄志宁、宋淑文、聂炎炎、卢应红、姜雷、高龙、顾盼、刘群林、高红影、
朱钇蓉、唐文金。
警示─使用本文件的人员应有正规实验室工作
CCS Y 43
中华人民共和国国家标准
GB/T 44364—2024
牙膏中丙烯酰胺的测定 高效液相色谱串联质谱法
Determination of acrylamide in toothpaste—
High performance liquid chromatography tandem mass spectrometry
2024-08-23 发布2025-03-01 实施
国家市场监督管理总局
国家标准化管理委员会发 布
目 次
前言 ····································································································· Ⅲ
1 范围 ·································································································· 1
2 规范性引用文件 ······················································································ 1
3 术语和定义 ··························································································· 1
4 原理 ·································································································· 1
5 试剂和材料 ··························································································· 1
6 仪器设备 ······························································································ 2
7 试验步骤 ······························································································ 2
7.1 试样溶液的制备 ················································································· 2
7.2 测定 ······························································································ 2
7.3 标准工作曲线绘制 ··············································································· 3
7.4 试样测定 ························································································· 3
7.5 空白试验 ························································································· 4
8 结果计算 ······························································································ 4
9 回收率 ································································································ 4
10 精密度 ······························································································· 4
11 检测限和定量限 ····················································································· 4
附录A （资料性） 丙烯酰胺标准物质/标准样品及内标信息 ·········································· 5
附录B （资料性） 丙烯酰胺及其内标标准溶液的多反应监测色谱图 ································· 6
前 言
本文件按照GB/T 1.1—2020《标准化工作导则 第1 部分：标准化文件的结构和起草规则》的规
定起草。
请注意本文件的某些内容可能涉及专利。本文件的发布机构不承担识别专利的责任。
本文件由中国轻工业联合会提出。
本文件由全国口腔护理用品标准化技术委员会（SAC/TC 492）归口。
本文件起草单位：苏州世谱检测技术有限公司、苏科世谱生物技术（苏州）有限公司、苏州质量检
测科学研究院、苏州市科耐瑞检测技术有限公司、广州舒客实业有限公司、广州质量监督检测研究院、
黑龙江省轻工科学研究院、无限极（中国）有限公司、福建爱洁丽日化有限公司、柳州两面针股份有限
公司、重庆登康口腔护理用品股份有限公司、浙江方圆检测集团股份有限公司、河北省食品检验研究
院、江苏省产品质量监督检验研究院、江苏省食品药品监督检验研究院、完美（广东）日用品有限公
司、清华大学、深圳大学、海南大学、苏州大学、常州大学、常州市食品药品纤维质量监督检验中心、
苏州市药品检验检测研究中心、山东华素健康护理品有限公司。
本文件主要起草人：张岩、卢剑、方方、何霜、朱丹丹、郑卫、结莉、李建祥、刘斌、秦天依、
叶竹洪、刘文玉、陈敏珊、高艳、蔡丽萍、胡永志、张环、杨铭、肖俊芳、代丹、陈晓珍、郭新东、
王怡、黄金凤、张迎阳、黄志宁、宋淑文、聂炎炎、卢应红、姜雷、高龙、顾盼、刘群林、高红影、
朱钇蓉、唐文金。
警示─使用本文件的人员应有正规实验室工作